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Carbon-coated Li2MnSiO4 powders as the active materials for the cathode were synthesized by planetary ball milling and solid-state reaction, and their phase formation behavior and charge-discharge properties were investigated. Calcination temperature and atmosphere were controlled in order to obtain the β-Li2MnSiO4 phase, which was active electrochemically, and the carbon-coated Li2MnSiO4 active material powders with near single phase β-Li2MnSiO4 could be fabricated. The particles of the synthesized powders were secondary particles composed of primary ones of about 100 nm size. The carbon incorporation was essential to enable the Li ions to be inserted and extracted from Li2MnSiO4 active materials, and the initial capacity of 192 mAh/g could be obtained in the Li2MnSiO4 active materials with 4.8 wt% of carbon.

journal of the korean electrochemical society/jeongi hwahag hoeji

Phase Formation Behavior and Charge-discharge Properties of Carbon-coated Li&lt;sub&gt;2&lt;/sub&gt;MnSiO&lt;sub&gt;4&lt;/sub&gt; Cathode Materials for Lithium Rechargeable Batteries