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Methanol electro oxidation on the surface of carbon paste modified by NiCl2/6H2O was studied in 1 M NaOH by potentiostatic and potentiodynamic methods. Ni/C catalyst by the concentration of 5% Ni showed about twice higher electro catalytic activity than Ni metal. The amount of monolayer’s on the surface of electrode is almost one order higher for Ni/C than Ni electrode. The kinetic parameters and the diffusion coefficient of methanol were derived from chronoamperometry (CA) and electrochemical impedance spectroscopy (EIS) measurements.

Physioelectrochemical Investigation of Electrocatalytic Activity of Modified Carbon Paste Electrode in Alcohol Oxidation as Anode in Fuel Cell