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Protonated layered perovskite compounds, HLaTiO4 and H0.34Na0.66LaTiO4·0.59H2O, were prepared from n = 1 Ruddlesden-Popper phase, NaLaTiO4, by the ion-exchange/intercalation reaction. Photocatalytic activities of HLaTiO4 and H0.34Na0.66LaTiO4·0.59H2O for H2 evolution from aqueous methanol solutions were studied. Anhydrous protonated form, HLaTiO4, showed higher photocatalytic activity than hydrous protonated form, H0.34Na0.66LaTiO4·0.59H2O. In a series of HxNa1-xLaTiO4·yH2O, it was considered that the influence of the distortion of TiO6 octahedra in the perovskite layer on the photocatalytic activities was greater than that of the presence of interlayer water molecules.

nihon ion kōkan gakkaishi/nihon ion koukan gakkaishi

Photocatalytic Activities of Protonated Layered Perovskite Compounds, HLaTiO4 and H0.34Na0.66LaTiO4 0.59H2O, Formed by Ion-exchange/intercalation Reaction