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A layered perovskite type oxide, HCa2Nb3O10, can incorporate mono- and divalent metal ions from aqueous solution. n-Pentylamine intercalates into the interlayer of HCa2Nb3O10 and the resulting oxide had an excellent reactivity for metal ions such as Cs+, Ca2+ or Sr2+. The mechanism of the intercalation of the metal ions into the hydrophobic interlayer in aqueous medium was studied.

Ion-Exchange Reaction of n-Pentylamine-Intercalated Layered Perovskite with Alkali and Alkaline Earth Metal Ions in Aqueous Solution