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The search for organocatalysts, i.e., small chiral molecules that are able to act as catalysts in enantioselective transformations, has received extensive attention, because of the potential for savings in cost, time and energy, easier experimental procedures, and reductions in chemical waste. 1 The aldol reaction is one of the most widely used reactions for C–C bond formation yet it has several drawbacks from an environmental standpoint, and this makes it an ideal candidate for organocatalysis. 2

Investigation of proline derivatives for the efficient organocatalysis of an Aldol type reaction in supercritical CO2