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The benzo[b]thiophene functionalization with benzyl groups at C-3 has been a synthetic challenge. Indeed, up to the date, few efforts have been successful in the achievement of this goal, and all of them involving drastic experimental conditions 1,2 . In this opportunity, trying to synthesize new benzo[b]thiophene frameworks, we inform the nonexpectable obtaining of benzo[b]thiophene dimers linked by a C-3 bond. In this sense, we think that this interesting experimental finding could lead to develop a new method to synthesize 3substituid benzo[b]thiophene with different kinds of benzyl alcohols.

Benzo[b]thiophene dimerization: A promising experimental finding directed to the C-3 functionalization with aryl alcohols.