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Recent progress in crystal engineering and crystallography has revealed many features of organic reactions performed in the solid state. The direct observation of a continuous change in the crystal structures of reactant molecules during the reactions in the crystalline state can give us valuable information. In this review article, we describe our recent studies on the mechanism of the solid-state organic reactions including EZ-photoisomerization, [2 + 2] photodimerization , and topochemical polymerization of muconic esters as the 1,3-diene monomers . The direct observation of molecular motion in the crystals during single crystal-to-single crystal transformation opens a new insight for understanding the mechanism of solid-state reactions and also the design of new functional solid materials.

Mechanistic Analysis of Solid-State Reactions by the Direct Observation of Crystal Structures