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Ethyl octyl sulfide was prepared by the reaction of 1-octanethiol with ethyl bromide in the presence of quaternary ammonium halide. The appropriate quaternary ammonium salt such as (n-C12H25) 3N+C2 H5Br- was found to be effective as the phase-transfer catalyst and the sulfide was obtained almost quantitatively in about 15 minutes.

Synthesis of Ethyl Octyl Sulfide in the Presence of Quaternary Ammonium Salt as Phase-transfer Catalyst