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The eight coordinated yttrium(lll) complex Y(tpb) 3 (H 2 O) 2 (Htpb=4,4,4-Trifluoro-1-phenyl-l,3-butane-dione) has been synthesized and structurally characterized by X-ray diffraction method. The coordination polyhedron of Y(tpb) 3 (H 2 O) 2 has a dodecahedron. The angle between two trapezia, Y-O2-O1-O5-O6 and Y-O4-O3-O8-O7, is 89.59°. The 01-05 and 03-08 distances are 2.965 and 2.995 A whereas the 02-06 and 04-07 distances are 4.256 and 4.403 A.

Structural Characterization of the Eight-Coordinated Dodecahedral Y(tpb)3(H2O)2

Structural Characterization of the Eight-Coordinated Dodecahedral Y(tpb)₃(H₂O)₂