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While arachno tetraosmium carbo-nyl boride cluster has a framework derived from anoctahedron with two adjacent equatorial vertexesremoved and another arachno pentaosmium carbo-nyl boride cluster has a framework that is basedupon a pentagonal bipyramidal structure from whichtwo nonadjacent equatorial vertexes have beenremoved, the framework of hexaosmium boridecluster which does not confirm to electron countingrule can be viewed as being derived from a pentag-onal bipyramid with one equatorial vertex removed.However, these clusters were obtained from thethermolysis of (µ-H)

journal of the korean chemical society

Improved Synthesis of Tetra- and Hexaosmium Carbonyl Boride Cluster HOs4(CO)12BH2and H3Os6(CO)16B