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Since Vecht and Quddus have reported the preparation of alkaline earth sulfides by using the reaction between alkaline earth alkoxides and H 2 S in 1976, a thio sol-gel process has been reported for the synthesis of metal sulfides using alkoxides or thiolates. The thio sol-gel process in which metal alkoxides act as the metal source uses H 2 S for a thiolysis reaction similar to H 2 O for the hydrolysis reaction in the conventional sol-gel process as follows:

Thio Sol-Gel Approach to An Octanuclear Titanium(IV) Cluster Compound