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The smallest ketenimine and hydrogen cyanide N-methylide ( and ) are provided from the argon/acetonitrile matrix samples exposed to radiation from laser ablation of transition-metals. New infrared bands are observed in addition to better determination of the vibrational characteristics for the previously reported bands, and the substituted isotopomers ( and ) are also generated. Density functional frequency calculations and the D and isotopic shifts substantiate the vibrational assignments. is probably produced through single-step conversion of , whereas through two-step conversion via 2H-azirine. Inter-conversions between these two products evidently do not occur during photolysis and annealing.

bulletin of the korean chemical society

Matrix Infrared Spectra and DFT Computations of CH2CNH and CH2NCH Produced from CH3CN by Laser-Ablation Plume Radiation