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E-mail: kimjn@chonnam.ac.krReceived October 3, 2012, Accepted October 19, 2012An efficient synthesis of phospha-Morita-Baylis-Hillman adducts was carried out in good yields via theMichaelis-Arbuzov reaction of the DABCO salts of MBH bromides. Instead of a DABCO salt, a phosphoniumsalt could be effectively used for some substrates which showed some problems in the presence of DABCO. Key Words : Phospha-Morita-Baylis-Hillman adducts, Michaelis-Arbuzov reaction, DABCO salt, AllylicphosphonatesIntroductionThe preparation of alkyl phosphonates was carried outmost frequently using alkyl halides and trialkyl phosphitesvia the Michaelis-Arbuzov reaction.

An Efficient Synthesis of Phospha-Morita-Baylis-Hillman Adducts via Michaelis-Arbuzov Reaction of the DABCO Salt of Morita-Baylis-Hillman Bromide