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In commercial DMT 1 hasbeen synthesized from p-xylene in air oxidation followed byesterification (Figure 1). In this process, partial oxidation ofxylene gave rise to major by-products MFB (methyl 4-form-ylbenzoate, (2)) and MMB (methyl 4-methylbenzoate, ( 3)).After separation of DMT 1 by distillation under reducedpressure, residues containing DMT 1, MFB 2, and MMB 3with 14%, 80%, and 6%, respectively have been disposed byopen burning/detonation. The use of open burning/detonationis becoming unacceptable due to public concern and environ-mental regulations. Therefore, the chemical conversionstudy of MFB 2 to higher value products would be highlydesirable.

Development on Recovery of MFB from Industrial Waste without Second Pollution