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) hybrid material was synthesized through a facile one-potsolvothermal method and used as the adsorbent for the preconcentration of some phthalate esters (dimethylphthalate, diethyl phthalate, diallyl phthalate, diisobutyl phthalate and benzyl butyl phthalate) in water samples.The effects of the adsorbent dosage, extraction time, the solution pH and salinity on the adsorption of thephthalate esters (PAEs) were investigated. The magnetic nanocomposite adsorbent could remove and enrichthe PAEs from water samples efficiently. After the adsorption, the analytes were desorbed and then determinedby high performance liquid chromatography-ultraviolet detection. Under the optimum conditions, theenrichment factors of the method for the analytes were in the range from 161 to 180. A linear response withpeak area as the quantification signal was observed in the concentration range from 0.5 to 100 ng mL

bulletin of the korean chemical society

Extraction of Phthalate Esters in Environmental Water Samples Using Layered-Carbon Magnetic Hybrid Material as Adsorbent Followed by Their Determination with HPLC