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Cyanosilylation of carbonyl compounds is an efficient procedure for the synthesis of silylated cyanohydrins, which are readily converted to several significant building blocks such as α-hydroxy acids, α-hydroxy aldehydes, 1, 2 diols, α-amino alcohols etc. In view of the importance of cyanohydrins, much attention has been focused on the development of practical methods for the synthesis of cyanohydrins. Among them, the cyanosilylation of carbonyl compounds using trimethylsilyl cyanide (TMSCN) is widely utilized for the synthesis of cyanohydrins. Several reagents including Lewis acids, Lewis bases, metal alkoxides, bifunctional catalysts, iodine and inorganic salts have been found to effectively transfer the cyano group from TMSCN to carbonyl compounds. Various types of Lewis acids such as AlCl3, 3

Efficient, Rapid and Solvent-free Cyanosilylation of Aldehydes and Ketones Catalyzed by SbCl3

Efficient, Rapid and Solvent-free Cyanosilylation of Aldehydes and Ketones Catalyzed by SbCl₃