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-(4-tosyloxy-methylcyclohexane)carboxamide, prior to the fluorination was quite inefficient with the low overall yield for the development of radiopharmaceutical due to the significant breakdown of amide bond, i.e., up to 70% of starting substrate, during the re-duction of carbomethoxy group toward WAY-100635 deriva-tive. Thereby, an efficient synthesis of

bulletin of the korean chemical society

An Efficient Synthesis of trans-N-{2-[4-(2-Methoxyphenyl)piperazinyl]ethyl}-N-(2-pyridyl)-N-(4-tosyloxymethylcyclohexane)carboxamide, A Precursor of [18