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Reduction of carbonyl compounds such as aldehydes, ketones, α,β-unsaturated enals and enones, α-diketones and acyloins was carried out readily with NaBH 3 CN in the presence of wet SiO 2 as a neutral media. The reactions were performed at solvent-free conditions in oil bath (70 - 80 °C) or under microwave irradiation (240 W) to give the product alcohols in high to excellent yields. Regioselective 1,2-reduction of conjugated carbonyl compounds took place in a perfect selectivity without any side product formation.

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Wet SiO<sub>2</sub>As a Suitable Media for Fast and Efficient Reduction of Carbonyl Compounds with NaBH<sub>3</sub>CN under Solvent-Free and Acid-Free Conditions

Wet SiO2As a Suitable Media for Fast and Efficient Reduction of Carbonyl Compounds with NaBH3CN under Solvent-Free and Acid-Free Conditions

Wet SiO₂As a Suitable Media for Fast and Efficient Reduction of Carbonyl Compounds with NaBH₃CN under Solvent-Free and Acid-Free Conditions