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.We first tried to optimize the reaction variables such as type of working amides, amines, oxidants, solvents, and temperatures using some representative carboxamides and triethylamine as test substrates (Table 1). With the employment of iodosylme-sitylene as a stoichiometric oxidant, the reaction turned out to be quite sensitive to the choice of amides examined. For in-stance, when benzamide was allowed to react with triethylamine in benzene,

Metal-Free Conversion of Carboxamides to Ureas Using Tertiary Amines and Iodosylmesitylene