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2 163.8 3 6.20 (d, 9.5) 111.9 C-2, C-4, C-10 4 7.84 (d, 9.5) 146.7 C-2, C-9 5 7.33 (d, 8.5) 128.5 C-7, C-9 6 6.84 (d, 8.5) 114.8 C-8, C-10 7 161.5 8 114.1 9 155.4 10 113.3 1′ 3.06 (dd, 7.5, 13.5) 3.16 (dd, 6.0, 13.5) 30.2 C-7, C-9, C-3′ 2′ 4.44 (dd, 6.0, 7.5) 76.3 C-8, C-4′, C-5′ 3′ 148.6 4′ 4.68 br s; 4.72 br s 111.4 C-2′, C-5′ 5′ 1.86 s 17.8 C-2′, C-4′ 2′′ 163.9 3′′ 6.18 (d, 9.5) 112.5 C-2′′, C-4′′, C-10′′ 4′′ 7.83 (d, 9.5) 146.2 C-2′′, C-9′′ 5′′ 7.45 (d, 8.5) 130.8 C-7′′, C-9′′ 6′′ 6.82 (dd, 2.5, 8.5) 114.6 C-8′′, C-10′′ 7′′ 163.2 8′′ 6.72 (d, 2.5) 103.5 C-6′′, C-10′′ 9′′ 157.3 10′′ 113.4 NMR data were obtained in 500 MHz for H and 125 MHz for C, respectively. Overlapped signals.

Limodissimin A: A New Dimeric Coumarin from Limonia acidissima