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While the dearylative chlorination reaction using hydrogen chloride requires a strong Lewis acid catalyst such aluminum chloride as a catalyst (Route B in Scheme 1). In the reduction steps of both routes, excess amount of lithium aluminum hydride is required and the lot of complexes of lithium aluminum halides (LiAlH

Dephenylation of Decaphenylcyclopentasilane with HCl Catalyzed by Aluminum Chloride: Facile Synthetic Route to Cyclopentasilane