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-butoxyaluminum hydrides. Using the best reac-tion condition from the experimental results, we appliedthese reducing agents for the synthesis of aldehydes from thevarious tertiary amides, respectively. The results for repre-sentative tertiary amides are summarized in Table 2.As shown in Table 2, both LDBBA and SDBBA weregood to convert tertiary amides to the corresponding alde-hydes. Thus, various aromatic amides examined possessingelectron-withdrawing or electron-donating groups are readi-ly converted to the corresponding aldehydes. A simplealiphatic and heterocyclic amide is also readily reduced toaldehydes in high yields.The utility of metal diisobutyl-

Reducing Characteristics of Metal Diisobutyl-t-butoxyaluminum Hydrides for Tertiary Amides