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seems to be obtain-ed because of higher affinity of the Cl atoms toward the Hgatom than that of the ether O donors in the ring cavity. Thebond angles around the Hg atom, (S,Cl)-Hg-(S,Cl), varyfrom 80.3(1) (S1-Hg-S2) to 131.6(1)° (S2-Hg-Cl1). Theselarge deviations are due to formation of the pentagonal ringvia Hg-S bonds. The ethylene unit between S1 and S2 isdisordered over two positions with occupancies of 0.54 [C9-C10] and 0.46 [C9'-C10'] (dashed-lines).

bulletin of the korean chemical society

Discrete and Continuous Soft Metal Complexes of O2S2and NO2S2Macrocycles with Endo- or Exo-Coordination Mode