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The reactions of mercury(II) chloride with O 3 S 2 -donor macrocyclic ligands with (L 1 ) and without (L 2 ) dibenzo-subunit afforded respective exo- (1) and endo-coordinated (2) complexes depending on the ring rigidity of the ligands. From the X-ray crystal structures and comparative NMR studies for the complexes 1 and 2, it is confirmed that the resulting species with different coordination modes exist not only in solid state but also in solution state.

Endo- and Exo-Coordinated Mercury(II) Complexes of O3S2Macrocycles: Effect of Dibenzo-Substituents on Coordination Mode

Endo- and Exo-Coordinated Mercury(II) Complexes of O₃S₂Macrocycles: Effect of Dibenzo-Substituents on Coordination Mode