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All reactions were carried out under an inert atmosphereof argon. TLC was conducted on E. Merck 60 F254aluminum backed silica gel plates (0.2 mm) with afluorescent indicator. Developed plates were visualizedunder UV light, with iodine staining, or by dipping in 2.0%phosphomolybdic acid solution and then heating. Flashcolumn chromatography was performed using Merck silicagel 60 (230-400 mesh) under positive pressure of airaccording to the procedure of Still.

A short Synthesis of Trimebutine, 2-Dimethylamino-2-phenylbutyl3,4,5-trimethylbenzoate