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On theother hand, synthesis of α-azidoketones directly startingfrom ketones has been by far less explored. To our bestknowledge, the only previous example of α-azidation of on of i t ac re e omh r our grou t p byd f porte e r ones was t e k α-( p -nitrobenzenesulfonyl)oxy ketone intermediates with sodiumazide in acetonitrile.

Efficient Preparations of α-Azidoketones and α-Thiocyanatoketones via α-Sulfonyloxy Aryl Ketone Intermediates in Ionic Liquid