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Department of Chemistry, and Research Center of Bioactive Materials, College of Natural Science, Chonbuk National University, Dukjindong 664-14, Chonju 561-756, KoreaReceived November 14, 2003As diverse synthetic precursors of cyclic adenosine diphosphate ribose (cADPR), several adenosine derivativesin which azido or amino group is introduced at 2'- or 3'-position of the sugar moiety of adenosine were preparedfrom readily available adenosine via conventional protocols. These synthetic sequence employs very efficientreactions conditions that proceed at or below ambient temperature with actual yields of >80% for eachindividual step. Key Words : Cyclic adenosine diphosphate ribose (cADPR), 2' (and 3')-Amino (and azido)- 2' (and 3')-deoxy-adenosineIntroductionCyclic adenosine diphosphate ribose (cADPR, 1) is anaturally occurring cyclic nucleotide and a general mediatorinvolved in Ca

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A Convenient and Versatile Synthesis of 2' (and 3')-Amino (and azido)-2' (and 3')-deoxyadenosine as Diverse Synthetic Precursors of Cyclic Adenosine Diphosphate Ribose (cADPR)