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In refluxing toluene, EPZ10 was found to be the mostreactive among three catalysts, giving the product in 84%isolated yield within 6 h. In contrast, the classical Biginellicondition (cat. HCl in EtOH, reflux, 18 h) gave 80% yield.The solvent effect was studied in the case of EPZ10-catalyzed reaction (Table 1). Clearly, toluene was a muchbetter solvent than other solvents tested in terms of yields.Lower boiling solvent (dichloromethane), protic solvent(EtOH) and Lewis basic solvents (THF, CH

Envirocat EPZ10: A Recyclable Solid Acid Catalyst for the Synthesis of Biginelli-type 3,4-Dihydropyrimidin-2(1H)-ones