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NaBH 4 with catalytic amounts of MoCl 5 can readily reduce a variety of carbonyl compounds such as aldehydes, ketones, acyloins, α-diketones and conjugated enones to their corresponding alcohols in good to excellent yields. Reduction reactions were performed under aprotic condition in CH 3 CN at room temperature or reflux. In addition, the chemoselective reduction of aldehydes over ketones was accomplished successfully with this reducing system.

A Mild and Convenient Method for the Reduction of Carbonyl Compounds with NaBH4in the Presence of Catalytic Amounts of MoCl5

A Mild and Convenient Method for the Reduction of Carbonyl Compounds with NaBH₄in the Presence of Catalytic Amounts of MoCl₅