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, a new precursor for the oxidative decarbonylation reaction, was synthesized in high yield by the one-electron oxidation reaction of . was structurally characterized, showing a dimeric nature with long (3.321 ) Mo-Mo bonding. Reaction of with sulfur gave the completely decarbonylated product (). The ligand substitution of the terminal sulfur ligands in to oxygen ligands was carried out with the use of PhIO to give (). The structures of and were also studied.

Oxidation of Tricarbonylmolybdacarborane.3.?A New Entry to the First Examples of Sulfido-Bridged Dinuclear molybda(V)carboranes