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, Z = 4, R = 0.0589) is a single-strand. The single strands are connected via the trifluoroacetateanions in a double-bridge, resulting in a typical molecular chicken-wire. The trifluoroacetate anion as aconnector appears to be primarily associated with its moderately coordinating ability. Their structural featureshave been discussed based on the anion exchangeability. Thermal analyses indicate that the compounds arestable up to approximately 200 oC. Key Words : Bridged anions, Silver(I) complexes, Bipyridine analogs, Coordination polymersIntroductionUntil recently, rational control of molecular frameworksvia weakly coordinating (counter)anions has been rare dueto the less effective electrostatic binding interactions. Studieson the anionic features such as negative charge, size, a widerange of geometries, significant solvent effects, and pHdependence show that some anions directly and indirectlyplay crucial roles in the construction of designed molecularbuildings.

Anions as Connectors for Higher Dimensions. Silver(I) Trifuoracetate with 3,3'-Oxybispyridine vs 3,3'-Thiobispyridine