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EDDAforms α-cis and β-cis isomers with vanadium(V) whileEDTA forms only the α-cis isomer with vanadium(V). Thesteric hindrance makes stable the α-cis form of the isomersbecause the substitution of an acetate group on nitrogenincreases steric bulk.In this paper we report the synthesis of a new vanadium(V) complex, triammonium (propylenediaminetetraacetato)-dioxovanadate(V) monohydrate, as well as its crystal struc-ture determined by X-ray crystallography. Propylenedi-aminetetraacetate (PDTA) is similar to EDTA in structure.PDTA has an asymmetric carbon on ethylenic backboneaccording to the substitution of a methyl group, while EDTAhas a symmetric structure. Experimental SectionMaterials . All reagent grade chemicals were used withoutfurther purification. Ammonium metavanadate (NH

Synthesis and Crystal Structure of Triammonium(Propylenediamonetetraacetato)dioxovanadate(V) Monohydrate Complex