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A set of Ni 0.5 Zn 0.5 Fe 2 O 4 samples were prepared by citrate precursor route to investigate the growth mechanism and its effect on cationic distribution. Following the information from DTA–TGA analysis, samples were annealed at 550 °C, 700 °C and 750 °C. Magnetization and Mossbauer studies suggest that initially the cationic distribution deviates from its normal preferences but it gets back to the normal preference at a temperature around 675 °C. It has been found that size onset for having the bulk cation configuration exclusively depends on the composition.   Keywords : Mossbauer Spectroscopy; Ferrite; Nanoparticles, Cationic distribution   International Journal of Engineering, Science and Technology , Vol. 2, No. 8, 2010, pp. 104-109

Cation distribution of Ni<sub>0.5</sub>Zn<sub>0.5</sub>Fe<sub>2</sub>O<sub>4</sub> nanoparticles