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A convenient and more efficient method for the preparation of 1,6-bis(2-pyridyl)-2,5-bis(2-hydroxy-3-formyl-5-methyl benzyl)-2,5-diazahexane, L 1 H 2 and 1,7-bis(2-pyridyl)-2,6-bis(2-hydroxy-3-formyl-5-methyl benzyl)-2,6-diazaheptane, L 2 H 2 are described. The ligands were prepared by reaction of two moles of 3-(chloromethyl)-2-hydroxy-5-methyl benzaldehyde with a mole of N,N'-bis(2-pyridyl)dopamine in THF at ambient conditions in high yield (75-80%) . KEY WORDS : Dicompartmental ligand, Synthesis, Phenol-based ligand, Acyclic ligand Bull. Chem. Soc. Ethiop. 2010 , 24(1), 151-155.

bulletin of the chemical society of ethiopia

&lt;b&gt;A convenient and efficient one-step method for the synthesis of dicompartmental ligands with hexa- and tetradentate coordination sites&lt;/b&gt;