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The reaction of equimolar amounts of ( n -Bu 4 N)[ReOCl 4 ] and 2-(1-ethanolthiomethyl)-1-methylimidazole (Htmi) in acetonitrile yielded cis -[ReOCl 2 (tmi)]. An X-ray diffraction study shows that tmiˉ coordinates as a uninegative N,S,O-tridentate ligand to give distorted octahedral geometry around the rhenium(V) ion. The three donor atoms occupy a triangular face in an octahedron, with the alcoholate oxygen coordinated trans to the oxo group. KEY WORDS: Oxorhenium(V), N,S,O-tridentate, Imidazole Bull. Chem. Soc. Ethiop. 2007 , 21(1), 75-81.

<b>Synthesis and crystal structure of an oxorhenium(V) complex containing a tridentate imidazole ligand</b>