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In this study, three-dimensional bismutite Bi2O2CO3 nanoparticels (BSC NPs) have been synthesized through a facile hydrothermal treatment under mild conditions. The reaction temperatures and NaOH concentration have a vital influence on the physical and photocatalytic properties of the obtained BSC NPs. The crystal structure, morphology, chemical composition, specific surface area and photoresponse of as-obtained catalysts were characterized by X-ray diffraction, Scanning electron microsprctrosopy, Energy-dispersive spectroscopy, N2 adsorption/desorption isotherms and UV-Vis spectra, respectively. Furthermore, Rhodamine 6G was used as model reaction to evaluate the photocatalytic activity of BSC NPs. As a result, there was no obvious effect of hydrothermal reaction temperature and NaOH concentration on phase structure and UV-visible light response; while the morphology, BET surface area and photoactivity were affected by hydrothermal reaction temperature and NaOH concentration.

open journal of physical chemistry

The Effect of Fabrication Conditions on the Morphology and Photocatalytic Activity of Bismutite Bi&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt;O&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt;CO&amp;lt;sub&amp;gt;3&amp;lt;/sub&amp;gt; Particles