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Cu(OTf)2(Py)4 mediated radiofluorination of the boronate esters of ethyl benzoyl and phthaloylglycinates (11 and 16) using 10 mol% of the copper complex following the literature procedure did not provide the fluorinated products. However, the addition of Cu(OTf)2resulted in the radio-fluorination of the boronate esters 11 and 16 to obtain ethyl 4-[18F]fluorobenzoyl glycinate, 17, (48%) and ethyl 3-[18F]phthaloylglycinate (41%) respectively.

natural science

Effect of Added Cu(OTf)&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt; on the Cu(OTf)&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt;(Py)&amp;lt;sub&amp;gt;4&amp;lt;/sub&amp;gt;-Mediated Radiofluorination of Benzoyl and Phthaloylglycinates