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Due to its importance in hydrogen production during the photolysis process of aqueous suspensions process, mixed TiO2/V2O5 metal-oxide semiconductors were prepared and subjected to crystal structure investigation using X-ray technique. The photoelectrochemical behavior of these TiO2/V2O5 was investigated by photolysis of aqueous suspensions of these oxides containing [Fe(CN)6]4-. X-ray diffraction analysis indicated that the TiO2 crystallites grow in the (1 0 1) direction, while The V2O5 crystallites seem to be growing in the (4 2 0) direction, with increasing concentration of V2O5. Photolysis studies show that photochemical activities that maintained the [Fe(CN)6]4/[Fe(CN)6]3- redox reversibility increased by increasing V2O5 up to 50% and then decreased at greater percentages. Aqueous nano systems used in these studies retained their stability as indicated by the reproducibility of their photo-catalytic activities

materials sciences and applications

Photoelectrochemical and Spectroscopic Studies of Colloidal Nano-Particles of Mixed TiO&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt;/V&amp;lt;sub&amp;gt;2&amp;lt;/sub&amp;gt;O&amp;lt;sub&amp;gt;5&amp;lt;/sub&amp;gt; Metal-Oxide Semiconductors