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The synthesis of novel isoxazolo[2,3-c][1,3,5]thiadiazepin-2-ones has been achieved in excellent yields by one-pot three-component Domino reaction without the production of toxic waste products by using p-toluene sulfonic acid (PTSA) as a Lewis acid catalyst. PTSA plays a crucial role in the success of the reaction, as well as for increasing reaction rate.

green and sustainable chemistry

One-Pot Three Component Domino Reaction for the Synthesis of Novel Isoxazolo[2,3-&amp;lt;i&amp;gt;c&amp;lt;/i&amp;gt;][1,3,5]Thiadiazepin-2-Ones Catalyzed by &amp;lt;i&amp;gt;PTSA&amp;lt;/i&amp;gt;—A Green Chemistry Approach