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It was confirmed that adherent film of polymer was formed onto steel electrodes by electrolysis of organic compounds under suitable conditions.Steel plate was usually used for both of anode and cathode; sometimes, carbon was used for anode. Ionization of iron was observed when steel was used for anode. Unsaturated carboxylic acids, aldehydes, trioxane, and vinyl compounds were used as monomers. The electrolysis was carried out under a constant current or under a constant applied voltage. This paper reports the weight and thickness of the film and its stability in water. The stability of the film in water especially depends upon the kind of supporting electrolytes. The coulomb efficiency for film formation and the quality of film depends upon the kinds of solvents and supporting electrolytes. The merits of this process consist in the direct formation of adherent polymer films for coating the cathode plate from monomers.

Formation of Polymer Film onto Steel Electrode by Electrolysis of Organic Compounds