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In the present article, high-pressure and high-temperature synthesis of new skutterudite compounds using a Kawai-type cell was reported. The structure and usage of the Kawai-type cell were explained. The first filled skutterudite compounds containing Ge atoms in the host network have been prepared at 7 GPa and 800°C in the Ln-Rh-Sb-Ge system, where Ln = La, Ce, Pr, and Nd. Some characteristic features of the Skutterudite structure were discussed.

High-Pressure Synthesis and Properties of New Filled Skutterudite Compounds Using a Kawai-Type Cell