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Mg:Al 3:1 hydrotalcite (Ht), used in catalytic quantities, promotes the generation of nitrosoalkenes, azoalkenes and nitrile oxides. These can be intercepted in situ by heterocycles and olefins in [4+2] and [3+2] cycloaddition reactions, producing dihydro-1,2-oxazines, tetrahydropyridazines and isoxazolines. The regeneration and reuse of Ht without loss of activity and the absence of organic solvent are the main advantages of this methodology.

Cycloaddition reactions of nitrosoalkenes, azoalkenes and nitrile oxides mediated by hydrotalcite