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Michael addition of heteroatomand carbon-centered nucleophiles on 7-oxanorborna-2,5-diene2-carboxaldehyde derivatives followed by a retro-Diels-Alder reaction allowed liquidand solidphase synthesis of a small library of α,β-unsaturated aldehydes. Emphasis should be put on the purity of the enals prepared on solid support, a purification step was not necessary.

Solid-phase cleavage by a thermal retro-Diels-Alder reaction: preparation of a small β-substituted α,β-ethylenic aldehydes library