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Cyclization of 1,7-(silyloxy)enynes with Ti(i-PrO)4 and n-BuLi yields 6-membered cyclic siloxanes in moderate to good yields. The reaction is highly diastereoselective (typical d.r.’s >15:1).

Highly diastereoselective titanium(II)-mediated cyclizations of 1,7-(silyloxy)enynes