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A mild and efficient method for the oxidative deprotection of trimethylsilyl and tetrahydropyran- yl ethers with Fe(NO3)3.9H2O in the presence of Fe(HSO4)3 in the absence of solvent at room temperature is reported.

arkivoc

Fe(NO3)3.9H2O / Fe(HSO4)3 : An efficient reagent system for the oxidative deprotection of trimethylsilyl and tetrahydropyranyl ethers in the absence of solvent