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Silica triflate was prepared as a stable white powder by the reaction of silica gel with trifluoromethylsulfonyl chloride at room temperature. This reagent efficiently catalyzed the onepot synthesis of 3,4-dihydropyrimidin-2-(1H)-ones and -thiones (DHPMs) under solvent-free reaction conditions in good to high yields.

Silica triflate as an efficient catalyst for the solvent-free synthesis of 3,4-dihydropyrimidin-2(1H)-ones