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Reaction of the title sulfone (1) with benzyl iodide at -78 degrees C in the presence of LiHMDS and using THF/DMPU as solvent affords a chromatographically separable mixture of the compounds 2-5 in a combined yield of 42%. These products have been subjected to comprehensive spectroscopic characterization and the structures of products 2 and 5 established through single-crystal X-ray analyses.

Spectroscopic and structural characterization of products arising from the base-promoted benzylation of 3-sulfolene