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Analysis of organometallic reaction mixtures by ElectroSpray Ionization Mass Spectrometry (ESI-MS) has permitted direct observation of Heck reaction intermediates using a 15-membered triolefinic macrocyclic palladium(0) complex as a recoverable catalyst. Knowledge has been gained of the role of the above- mentioned palladium complex in the Heck reaction by using arenediazonium salts.

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ESI-mass spectrometry as a tool for investigating the mechanistic role of a 15-membered triolefinic macrocyclic palladium(0) complex in the Heck reaction