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A tandem 5-exo-trig-vinyl-3-exo-radical cyclization-rearrangement reaction and its allylic radical version was developed (8 & 15 to 9 & 16 respectively) for the synthesis of DEF ring system of the nor-tritepene Pfaffic acid 1.

Synthetic studies towards the nor-triterpene pfaffic acid: Synthesis of DEF ring fragment via tandem radical cyclization rearrangement reactions