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Wang resin bound N-fluorenylmethoxycarbonyl (Fmoc) amino acids and dipeptides were efficiently converted into the corresponding N-tert-butoxycarbonyl (Boc) derivatives using two different “one-pot” procedures: potassium fluoride / di-tert-butyl carbonate and potassium fluoride / tert-butyl S-(4,6-dimethylpyrimidin-2-yl) thiolcarbonate.

Efficient and simple one-pot conversion of resin-bound N-Fmoc amino acids and dipeptides into N-Boc derivatives